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Malvern Instrument’s Spraytec laser diffraction system allows measurement of spray particle and spray droplet size distributions in real-time for more efficient product development of sprays and aerosols. It has been specifically designed to address the unique requirements for spray characterization and deliver robust, reproducible droplet size data.

Overview

Incorporating over 35 years of experience in spray applications, the Malvern Spraytec provides the data required to fully understand spray and atomization processes. It will:

  • Measurement across a wide size range (0.1 – 2000 microns) without requiring constant optics changes.
  • Resolve rapid changes in droplet size over time, by measuring up to 10,000 measurements a second.
  • Deliver accurate, concentration-independent results using a patented multiple scattering analysis.
  • Characterize wide spray plumes without risking optical contamination.
  • Simply reveal the dynamic changes in spray particle size through its unique size history analysis software.

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How it works

The Malvern Spraytec uses the technique of laser diffraction for measurement of the size of spray droplets and spray particles. It does this by measuring the intensity of light scattered as a laser beam passes through a spray. This data is then analyzed to calculate the size of the droplets that created the scattering pattern.

The Spraytec system is made up of the following main elements:

  • A transmitter module which contains the collimated laser light source used to illuminate the spray during a measurement.
  • A receiver module which can hold one of two lenses (300mm or 750mm) which focus any light scattered by the spray onto a series of detectors. These detectors accurately measure the intensity of light scattered by the spray droplets over a wide range of angles.
  • An optical bench which ensures the transmitter and receiver are aligned. The length of this can be changed in order to fit with different applications, with the longest bench being 2.5m long.
  • The Spraytec software which controls the system during the measurement process and analyzes the scattering data to calculate spray size distributions. The results are displayed as a ‘size history’ trend plot, allowing any changes in the droplet size over time to be instantly recognized.

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Specification

General

Principle
Laser Light Scattering.
Analysis
Mie and Fraunhofer scattering including a patented multiple scattering analysis.
Maximum Data acquisition rate
Rapid mode: 10kHz.
Continuous mode: 1Hz.
Maximum Measurement Time
Rapid mode: 30 seconds.
Continuous mode: 60 minutes.
Measurement Triggering
Internal: Based on transmission or light scattering levels.
External: Based on TTL input or simple switch trigger.
External Device Synchronization
Via 2 TTL trigger outputs.

Optics

Light Source
Max 4mW He-Ne Laser, 632.8nm.
Lens Arrangement
Fourier (parallel beam).
Lens Focal Length(s)
300mm and 750mm.
Measurement Working Range*
150mm at 0.5 µm, extending to greater than 1m above 5 µm.

Detector

Arrangement
36 element log-spaced array.
Angular range
0.015 – 17 degrees.**
Alignment
Automatic.

Sizing Performance

Size Range
300mm lens: 0.1 – 900 µm (Dv50: 0.5 – 600 µm).
750mm lens: 2 – 2000 µm (Dv50: 5 – 1600 µm).
Accuracy
Better than 1%.***
Repeatability
Better than 1%.***
Reproducibility
Better than 1%.***

Software

21CFR Par 11
Enables an operating mode that assists with ER/ES compliance.

System Compliance

Laser Class
Class 3R, IEC60825-1:2007 and CFR Chapter 1: Sub-chapter J: Part 1040 (CDRH).
Regulatory testing
CE / FCC compliant.
Meets requirements of the European Low Voltage directive.

Weight and dimensions

Laboratory systems
950mm optical bench: 950mmx550mmx610mm (36kg).
1400mm optical bench: 37kg 1400x550x610 (37kg).
Spray Facility Systems
950mm optical bench: 950mmx550mmx650mm (36kg).
1400mm optical bench: 1400x550x650 (37kg).

System

Supply Voltage
100/240 v, 50/60 Hz.
Product storage temperature
-20°C to +50°C.
Operational temperature range
+15°C to +40°C.
Humidity range
80% maximum for temperatures up to 31°C, decreasing linearly to 50% at 40 °C. Non-condensing.
Ingress Protection
IP65 when in normal use

Computer Specification (recommended)

Computer interface
At least 1 USB port required.
Operating System
Windows XP Professional (SP3 or higher).
Windows 7 professional (32bit or 64 bit).
Hardware Specification
Intel 2.8GHz Pentium IV Processor, 512GB RAM, 160GB HD, CD-ROM or DVD +/-RW drive, 17 inch Flat Panel Monitor.
Notes
*
This defines the maximum allowable distance between the far edge of the spray plume and the Spraytec receiver lens.
**
Lens dependent.
***
Relates to the measurement of the Dv50 for NIST-traceable latex standards. Sample dependent.

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Accessories

Nasal Spray Accessory Accurately positions nasal pump sprays at a known distance and angle relative to the Spraytec measurement zone. Can be used with most common automated actuator systems. More information
Inhaler and Nebulizer Accessory Designed to provide a rapid way of characterizing inhalers and nebulizer under controlled conditions. More information
Aerosol Positioning Accessory Provides a simple to use way of holding and positioning aerosol cans and sprays at a known distance from the Spraytec measurement zone. More information
Air Purge Accessory Reduces the risk of contamination of the Spraytec optics during the measurement of wide spray plumes. More information
Extraction Accessory HEPA-rated extraction system, designed to minimize user exposure to sprays and also ensure droplet and particle recirculation does not occur. More information
Wet Dispersion Accessory A cost effective wet sample dispersion unit designed for measuring samples in aqueous and non-aqueous liquids. More information

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Spraytec spray particle analyzers allow real-time particle size distribution measurements of sprays and aerosols.